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High Light: | metal analysis spectrometer,UV Visible Spectroscopy |
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Fully Automated Single Beam Flame & Graphite Atomic Absorption Spectrophotometer AA500FG
Features & Functions
AA-Win Pro software provides full control of the instrument and auto sampler with easy method change for each technique
Automatic 8 Hollow Cathode lamp turret controlled and optimized by the AA-Win Pro software. Operating lamp current and warm-up current can be individually controlled to eliminate drift commonly associated with lamp warming
D2 lamp background correction system fitted as standard to all configurations. High energy D2 lamp and adjustable beam splitter mirror are optimized by the AA-Win Pro software
Self reversal background correction system fitted as standard to all configurations. The high performance background system uses the same hollow cathode lamp as installed for the analysis. Minimum extra components are required and optical alignment is very simple. Self reversal can be used for any element at any wavelength making it extremely versatile.
High precision minimal optics ensures maximum light throughput to the computer controlled Czerny-Turner monochromator.
A universal auto sampler is available as an optional accessory which is conveniently mounted on the front of the AA500 instrument.
Absorption and Emission modes are standard features in the AA-Win Pro software as well as peak height, peak area, sequential and manual integration modes.
Flame Atomiser Features
The flame atomizer offers three flame options: Air/Acetylene is the standard configuration with the N2O/acetylene and Air/LPG as options.
Air/Acetylene
The Air/Acetylene flame uses a 100mm single slot burner for the standard configuration
The high sensitivity (Cu 2ppm>0.280Abs) is due to the efficiency of the fixed position glass nebulizer fitted as standard. An acid resistant replacement is available as an option.
The flame can be easily set from blue lean flame through stoichiometric to fuel rich by means of computer control
N2O/Acetylene
The N2O/Acetylene flame uses a 50mm single slot burner and is available as an optional extra.
This flame configuration is used to measure elements less prone to ionization such as Aluminum, Tin, Titanium, Calcium, Vanadium and Molybdenum.
Switching from Air/Acetylene to N2O/Acetylene to Flame Off is fully controlled by the AAWin Pro software
Air/Propane (LPG)
This flame uses a 3 slot burner and with the low pressure requirement it is also much safer to operate
Due to the low temperature of the flame it is ideal for analyzing alkali metals such as Potassium, Sodium and Lithium, especially when used in the emission mode.
Some remote areas of the world have difficulty obtaining Acetylene gas of a high enough purity to operate the flame correctly. LPG can give a real alternative and offer comparable results for most elements throughout the wavelength range.
Safety Features
Graphite Atomiser Features
The integrated Graphite Furnace Atomiser is available in two instrument configurations.
Safety Features
Argon gas pressure sensor
Water flow sensor
Over temperature sensor
Broken graphite tube protection
Applications:
Agricultural
Clinical
Environmental
Food
Metal
Mining
Geological
Pertrochemical
Pharmaceutical
Specifications:
Spectrometer System |
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Wavelength range |
190-900nm |
Light source |
Hollow cathode lamp (HCL), Deuterium Arc lamp (D2) |
Modulation |
Square wave pulse |
Modulation frequency |
100hz self reversal (SR) background, 400hz Deuterium Arc (D2) background |
Monochromator |
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Grating |
1800 grooves/mm diffraction grating |
Blazed wavelength |
250nm |
Focus |
300nm |
Bandwidth |
0.1, 0.2, 0.4, 1.0, 2.0, 5.0nm |
Scan mode |
Automatic |
Photometric type |
Single beam |
Wavelength accuracy |
+0.15nm |
Wavelength resolution |
0.2nm+0.02nm |
Wavelength reproducibility |
<0.05nm |
Baseline stability |
0.005A/30min |
Stray light |
≤0.12%T(220nm NaI, 340nm NaNO2) |
Background correction |
Deuterium Arc (D2) 1.0Abs, Self Reversal (SR) 3.0Abs |
Flame Analysis |
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Flame types |
Air/Acetylene, Nitrous Oxide/Acetylene, Air/Propane (LPG) |
Sensitivity (Cu) |
2μg/ml Absorption >0.280Abs |
Characteristic concentration |
Cu<0.02μg/ml, Ba<0.15μg/ml (N2O/Acetylene) |
Detection limit |
Cu<0.004μg/ml |
repeatability |
Cu<0.7% (Air/Acetylene Flame) Ba<1.0% (Nitrous Oxide/Acetylene Flame) |
Burner heads |
Titanium alloy |
Nebulizer |
High efficiency glass, Acid proof available as an option |
Pre-mix chamber |
Corrosion resistant |
Atomizer selection |
Automatic changeover (AA500FG), |
Safety features |
Burner identification, flame sensor, gas leak sensor, low gas pressure sensor, drain trap sensor, power loss protection |
Graphite Furnace Analysis |
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Graphite head |
Transversally heated |
Temperature range |
Ambient-2650℃ |
Heating program |
Up to 10 steps. Drying, Ashing, Atomization, Cleaning |
Feedback |
Voltage and optical temperature control feedback |
Sensitivity (Cu) |
50ng/m Absorption>0.40Abs |
Detection limit |
Cd<0.004ng/ml |
Repeatability |
Cu<2.0%, Cd<2.0% |
Graphite tubes |
Pyrolytically coated with platform |
Sample size |
Up to 20μl |
Graphite cooling |
Water circulator available |
Safety features |
Argon pressure sensor, water flow sensor, over temperature sensor, broken tube protection |
Data Processing |
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Operating program |
AA Win Pro software |
Analytical methods |
Flame AA, Flame AE, Graphite Furnace, Hydride Generation |
Readout Mode |
Continuous, manual, peak height, peak area |
calibrations |
Multi-standard calibration, standard addition, interpolation |
Data storage |
Analytical results, instrument and measurement parameters, signal profile, calibration curve |
Power Requirements |
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Main unit |
220Vac 50/60hz 200W |
Graphite power supply |
220Vac 50/60hz instantaneous power 5KW current rating |
Dimensions |
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Main unit |
110x54x54cm 75kg |
Graphite power supply |
50x54x54cm 70kg |
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The AA500 Atomic Absorption Spectrometer is a high performance automated instrument designed to meet the requirements of the modern laboratory. Due to its versatility and performance it can be used for a wide range of applications. The versatile instrument is available in three configurations:
AA500FG-The instrument is equipped with a flame atomizer and a graphite furnace atomiser. The positioning of which is fully controlled by the embedded computer system and AA-Win Pro software. Three flame options are available to the user with the Air/Acetylene being the standard configuration. This flame can be used for nearly all standard elements while the N2O/Acetylene and the Air/LPG (natural gas) are available as an option for the more demanding of elements. All three flame configurations offer coded burner for full safety protection. The graphite head is fixed into the optical path to maximize performance and eliminate drift. The temperature of the transversely heated graphite tube is accurately controlled by means of a precision feedback system. Pyrolytically coated platform tubes are supplied as standard to improve the performance and eliminate many analytical problems associated with this technique. The flame and graphite furnace can be changed over by a simple selection in versatile AA Win software.
Optional Accessories & Consumables
Coded nitrous oxide burner
Coded low temperature burner
Auto sampler
Hydride system
Air compressor
Water circulator
Hollow cathode lamp
Glass nebulizer
Graphite tube
O-ring
Pipette
Deuterium lamp
Photomultiplier tube
Contact Person: Miss. April Cao
Tel: 86 -10 -69910653
Fax: 86-010-69910516